SFC 2015 Scientific Program

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Oral Presentations

Mohammed Al-SavahGenentech, Inc.“Development of an Automated Two-dimensional Liquid Chromatography- Supercritical Fluid chromatography System”
Daniel ArmstrongUniversity of Texas at Arlington“Packed Column SFC: A Driving Force in Enantiomeric Separations”
Christine AurigemmaPfizer, Inc.“FastTrack SFC/HPLC Revisited: Lessons Learned from ImplementingSFC into the Medicinal Chemistry Laboratory”
Robert M. CampbellThe Dow Chemical Company“ Software Assisted Characterization of Complex Materials bySFC/MS”
Ruben DePauwVrije Universiteit Brussel“Extra-column band broadening effects in supercritical fluidchromatography: experimental measurements and theoreticalmodelling”
Vincent DesfontaineUniversity of Geneva“Evaluation of new stationary phase chemistries in sub-2μmand Core-Shell material for the analysis of basic compounds inSFC”
Alexandre Grand-Guillaume PerrenoudUniversity of Geneva“UHPSFC-QToF-MS as a first line analytical tool for naturalbioactive compound analysis”
Michael HicksMerck Research Laboratories“Evaluation of Analytical Chiral Supercritical Chromatographyfor GMP Activities in Pharmaceutical Development andManufacturing”
Chris HudallaProverde Laboratories“Development of an SFX Workflow for the Analysis and Preparationof Cannabis Based Natural Therapeutics”
Shane KastenUS Army Medical Research Institute of Chemical Defense“Crossroads between Chemical Warfare Nerve AgentCountermeasure Development and Chiral Supercritical FluidChromatography”
Jeffrey KiplingerAverica Discovery Sciences“Understanding the Real Value of Prep SFC Technology: ABetter Way to Look at Technology and the Design of the R&DProcess”
G. John LangleyUniversity of Southamption“Analysis of Oilfield Chemicals by UHPSFC-MS”
Ira Luirethe George Washington University“Ultra High Performance Supercritical Fluid Chromatographyfor the Analysis of Synthetic Cannabinoids”
Daniel MarkowitzJohnson Matthey Pharmaceutical Materials and Services“ Practical Scale Up Lessons for Supercritical Fluid ChromatographyTechnology Beyond the Lab”
John McCauleyWaters Corporation“The Decaffeination of Coffee Beans assisted by SupercriticalFluid Extraction, (SFE), Techniques”
Edgar NaegeleAgilent Technologies“Quantitative Determination of multi-Pesticide Residues inVegetables by Supercritical Fluid Chromatography Coupled toTriple Quadrupole Mass Spectrometry”
Hermes Licea PerezGlaxoSmithKline“Applications of Supercritical Fluid Chromatography (SFC) forChiral Metabolite Separations in DMPK Environment”
Donald PoeUniversity of Minnesota Duluth“ The Joule-Thomson Coefficient as a Criterion for EfficientOperating Conditions in SFC Using Fully Porous and SuperficiallyPorous Packings in Convective Air Environment”
Oleg PokrovskiyKurnakov Institute of General and Inorganic Chemistry“SFC Separations of Closely Related Compounds Not Based onHydrogen Bonding”
Gerard RosseDart Neuroscience LLC“ Maximizing Efficiency in Drug Discovery: SFC-MS as theTechnique of Choice for Small Molecules Purification”
Tohru ShibataDaicel Corporation“Achiral SFC on Polysaccharide-based CSP”
Abhijit TarafderWaters Corporation“ Effect of Density Gradient on Non-Linear Band Profiles inSFC”


Poster Presentations

Todd M. Anderson, Kenichiro TanakaShimadzu Scientific Inc., Columbia, MD, USA“Automated Chiral and Achiral Method Development by SFC”
Takeshi Bamba, Manako Ueno, YoshihiroIzumi, Yasuhiro Funada, Yosuke Iwata,Masami Tomita, Eiichiro FukusakiDept. Biotech., Grad. Sch. Eng., Osaka Univ., Osaka,JAPAN. Medical Institute of Bioregulation, Kyushu Univ.,Fukuoka, JAPAN. Shimadzu Co., Kyoto, JAPAN

“Development of an Online Supercritical Fluid Extraction-Supercritical Fluid Chromatography/Mass Spectrometry method for the Simultaneous and Rapid Analysis of Fat-Soluble Vitamins”

Alex Brien, Dave Leach, VictoriaCoulthard, Phil AbbottReach Separations, Nottingham, ENGLAND“An Automated Approach to Mixed Modifier Chiral Screening”
Geoffrey B. Cox, Christina Kraml

PIC Solutions, Media, PA, USA, Lotus Separations LLC, Princeton, NJ, USA

“Concentration, Isolation and Removal of Sample Impurities using Extraction-Injection in Preparative Supercritical Fluid Chromatography”

R. DePauw, K. Choikhet, G. Desmet, K.BroeckhovenVrije Universiteit Brussel, BELGIUM

“Volumetric Flow Rates in Supercritical Fluid Chromatography: At Which Reference Conditions?”

Peter Gidlund, Joakin HogblomAkzo Nobel Pulp and Performance Chemicals AB, Bohus,


“Exploring the Potentials of Using SFC as an Analytical Tool for Peptides”

Shawn C. Helmueller, Donald P. PoEUniversity of Minnesota Duluth, Duluth, MN USA

“Packed Column SFC at Low Outlet Pressures: The Pursuit of Adiabatic SFC”

Jason Hill, Andy Aubin, Abhijit TarafderWaters Corporation, Milford, MA, USA“Method Parameter Considerations in SFC Method Transfer”
Yoshihiro Izumi, Eiichiro Fukusaki,Takeshi Bamba

Medical Institute of Bioregulation, Kyushu Univ., Fukuoka,JAPAN. Dept. Biotech., Grad. Sch. Eng., Osaka Univ.,Osaka, JAPAN|

“Supercritical fluid chromatography tandem mass spectrometry: An alternative to LC/MS/MS for highly-sensitive and high-throughput analysis of multiresidue pesticides”

Marc Jacob, Richard Hodgson, MichaelKlein

Phenomenex LTD, Chesire, UNITED KINGDOM, PhenomenexInc. Torrance, CA, USA

“Novel Screening Approach for the Separation of Pharmaceutical Compounds Using Lux® Polysaccharide-Based Chiral Stationary Phases in SFC Mode”

Jinchu Liu, Mirlinda Biba, Ingrid MergelsbergMerck Research Laboratories, Rahway, NJ, USA

“Exploring the Application of Preparative SFC for Purification/ Separation of APIs and Intermediates at Merck”

Thomas Mahoney

Dr. Reddy’s Laboratories Ltd. – ChiroTech TechnologyCentre, Cambridge, UNITED KINGDOM

“Transitioning from Reversed Phase to Supercritical – Why Bother?”

Johanna Malm, Pernilla Korsgren, AnnikaLangbord Weinmann, Hanna Lee,Kristina OhlenAstraZeneca R&D, Molndal, SWEDEN

“Water as Additive in a Generic SFC Method Used in Preparative Scale”

Martina Noll-Borchers, Timo Hölscher1,Edgar Naegele, Markus Becker

SIM Scientific Instruments Manufacturer GmbH, Oberhausen,GERMANY, Agilent Technologies, Inc., Waldbronn, GERMANY

“SFC-FID for Determination of Aromatics in Diesel Fuels – FID Development Meeting the Requirements of ASTM D-5186”

Lucie Nováková, Katerina Plachká, LuciaChrenková, Michal Douša

Department of Analytical Chemistry, Faculty of Pharmacy,Charles University, Heyrovského 1203, Hradec Králové,CZECH REPUBLIC, Zentiva, k.s. Praha, U Kabelovny 130, 102 37 Praha 10, CZECH REPUBLIC

“Development of UHPSFC and UHPLC Methods For The Determination of Agomelatine and Its Impurities in Tablets”

J. Preston, Julissa Fernandez, Michael McCoy, Marc Jacob, William Farrell

Phenomenex Inc; Torrance, CA USA, Pfizer Global R&D; LaJolla, CA, USA“Chiral Screening on Polysaccharide Columns with SFC and Translating the Results to Liquid Chromatography”
Matthew PrzybycielES Industries, West Berlin, NJ, USA“SFC Analysis of Pharmaceuticals and Nutraceuticals Using SFC Optimized Stationary Phases”
Gerard Rosse, Yinong Zhang, Kim Kim DaoDart Neuroscience, LLC., San Diego, CA, USA“Novel Stationary Phases Optimized for UHPSFC-MS”
Jacquelyn RuncoWaters Corporation, Pittsburgh, PA, USA“Demonstrating an SFE-SFC Workflow to Isolate Target Flavor Compounds From Natural Products”
Lisa M. SchaffterSopheary K. Op, Abbvie, Worcester, MA, USA“Investigation of Traditional LC Scaling Methodology when Converting to Smaller Particle Size Columns in an SFC Environment and the Applicability of the “Density Variation” Rule for SFC in Gradient Method Scaling”
Jennifer Simeone, Paula Hong, Patricia R. McConvilleWaters Corporation, Milford, MA, USA“Recent Advances in SFC Instrumentation for the Development of High Efficiency Analytical Methods”
E.J. Sobkow, J. Kawabata, R. Spaegele, S. Nozawa, T. Adachi, N. KurodaYMC Co., LTD, DSM Nutritional Products, YMC America, Inc.“SFC Analytical Method Development for Vitamin D3 and Related Compounds”
Thomas Swann, Kenneth Berthelette, Jacob Fairchild, Jason HillWaters Corporation, Milford, MA, USA“Using Blends of Solvents and Additives to Enhance SFC Chiral Method Development Screening”
Kenichiro Tanaka, William Hedgepeth, Daisuke Nakayama, Hidetoshi Terada, Minori Nakashima, Tadayuki YamaguchiShimadzu Scientific Instruments, Inc., Columbia, MD, USA Shimadzu Corporation, Kyoto, JAPAN“A novel approach to cleaning validation for pharmaceutical manufacturing by online supercritical fluid extraction/supercritical fluid chromatography”
Takato Uchikata, Hidetoshi Terada, Yasuhiro Funada, Yoshihiro Izumi, Takeshi BambaShimadzu Corporation, Kyoto, JAPAN, Medical Institute of Bioregulation, Kyushu Univ., Fukuoka, JAPAN., Dept. Biotech., Grad. Sch. Eng., Osaka Univ., Osaka, JAPAN“Automatically extraction and analysis using on-line supercritical fluid extraction (SFE) / supercritical fluid chromatography (SFC) system”
Takato Uchikata, Takanari Hattori, Hidetoshi Terada, Chigusa Ichikawa, Yasuhiro Funada, Yayoi Ichiki, Miho Sakai, Takashi Ando, Yoshihiro Izumi, Eiichiro Fukusaki, Takeshi BambaShimadzu Corporation, Kyoto, JAPAN, Miyazaki Enterprise Promotion Organization, Miyazaki, JAPAN, Miyazaki Agricultural Research Institute, Miyazaki, JAPAN, Kushu University, Fukuoka, JAPAN, Osaka University, Suita, JAPAN“Fully automated on-line sample extraction and analysis of residual pesticides in agricultural products by using on-line SFE-SFC-MS”
Jennifer Van Anda, Siji JosephAgilent, Wilmington, DE, USA“Achiral and Chiral Metabolite Profiling Using Hybrid SFC/UHPLC System Coupled with Triple Quadrupole”
Jennifer Van Anda, Rick WikforsAgilent Technologies, Wilmington, DE, USA“A novel approach to cleaning validation for pharmaceutical manufacturing by online supercritical fluid extraction/supercritical fluid chromatography”
David Wechsler, Eric Bald, Beatrice David, Philippe JablonskiHoffman La Roche, Basel, SWITZERLAND“SFC Applications for Small Molecules in Medicinal Chemistry”
Yinong Zhang, Kim Kim Dao, Gerard RosseDart Neuroscience, LLC., San Diego, CA, USA“Chiral SFC Screening of a 896-Member Small Molecules Library”
Yinong Zhang, Irena Khachian, Kim Kim Dao, Gerard RosseDart Neuroscience, LLC., San Diego, CA, USA“Optimization of Flow Splitters for Preparative SFC-MS”